环孢霉素A

CyclosporineA (25mM, C6D6):  400MHz,  Quantum-I Plus , with broadband STM Probe

Structure of cyclosporine A

Figure 1 COSY 1024×256, 8 scans 

Figure 2 TOCSY, 1024×512, 8 scans

Figure 3 NOESY, 1024×512 , 16 scans

Figure 4 HSQC，1024×256, 16 scans

Figure 5 HMBC, 1024×256, 16 scans

Figure 6 1H-15N  HSQC, 1024×256, 16 scans

Figure 7 1H-15N HMBC, 1024×256, 16 scans

乙酸胆甾醇脂

Cholesteryl acetate (100 mM, CDCl3): 400MHz,  Quantum-I Plus , with broadband STM Probe

Structure of cholesteryl acetate

Figure 1 Normal 13C spectrum

Figure 2 DEPT135 spectrum

Figure 3 HSQC-TOCSY, 512×512, 32 scans

六氟丁醇

Hexafluorobutanol (100 uL, Acetone-d6):  400MHz,  Quantum-I Plus , with broadband STM Probe

Structure of hexafluorobutanol

Figure 1 1H-19F COSY: 1024×256, 4 scans